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LABOMATIC Instruments uv triggered preparative hplc
Uv Triggered Preparative Hplc, supplied by LABOMATIC Instruments, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/product/uv+triggered+preparative+hplc/uv+triggered+preparative+hplc/us11773070-709-30-35
Average 90 stars, based on 1 article reviews
uv triggered preparative hplc - by Bioz Stars, 2026-09
90/100 stars

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Liquid Chromatography with Mass Spectroscopy:

Article Title: Dihydrooxadiazinones
Article Snippet: Nuclear magnetic resonance (NMR) spectra were recorded on a Bruker (300 or 400 MHz 1H, 75 or 101 MHz 13C) spectrometer. .. Preparative LC-MS Methods: Unless otherwise noted compounds were purified using mass-triggered preparative HPLC (Waters Autopurificationsystem; Column: Waters XBridge C18 5μ 100×30 mm; DAD scan: 210-400 nm, flow: 150 mL/min) or UV triggered preparative HPLC (pump: Labomatic HD-5000 or HD-3000, head HDK 280, lowpressure gradient module ND-B1000; manual injection valve: Rheodyne 3725i038; detector: Knauer Azura UVD 2.15; collector: Labomatic Labocol Vario-4000; column: Chromatorex RP C-18 10 μm, 125×30 mm, flow: 70 mL/min) Acidic conditions: Eluent A: water+0.1 vol-% formic acid, Eluent B: acetonitrile+0.1 vol-% formic acid; Basic conditions: Eluent A: water+0.2 Vol-% aqueous ammonia (32%), Eluent B: acetonitrile; Experimental Section—General Procedures General Details All reactions were carried out under nitrogen (N2) atmosphere. ..

Purification:

Article Title: Dihydrooxadiazinones
Article Snippet: Nuclear magnetic resonance (NMR) spectra were recorded on a Bruker (300 or 400 MHz 1H, 75 or 101 MHz 13C) spectrometer. .. Preparative LC-MS Methods: Unless otherwise noted compounds were purified using mass-triggered preparative HPLC (Waters Autopurificationsystem; Column: Waters XBridge C18 5μ 100×30 mm; DAD scan: 210-400 nm, flow: 150 mL/min) or UV triggered preparative HPLC (pump: Labomatic HD-5000 or HD-3000, head HDK 280, lowpressure gradient module ND-B1000; manual injection valve: Rheodyne 3725i038; detector: Knauer Azura UVD 2.15; collector: Labomatic Labocol Vario-4000; column: Chromatorex RP C-18 10 μm, 125×30 mm, flow: 70 mL/min) Acidic conditions: Eluent A: water+0.1 vol-% formic acid, Eluent B: acetonitrile+0.1 vol-% formic acid; Basic conditions: Eluent A: water+0.2 Vol-% aqueous ammonia (32%), Eluent B: acetonitrile; Experimental Section—General Procedures General Details All reactions were carried out under nitrogen (N2) atmosphere. ..

High Performance Liquid Chromatography:

Article Title: Dihydrooxadiazinones
Article Snippet: Nuclear magnetic resonance (NMR) spectra were recorded on a Bruker (300 or 400 MHz 1H, 75 or 101 MHz 13C) spectrometer. .. Preparative LC-MS Methods: Unless otherwise noted compounds were purified using mass-triggered preparative HPLC (Waters Autopurificationsystem; Column: Waters XBridge C18 5μ 100×30 mm; DAD scan: 210-400 nm, flow: 150 mL/min) or UV triggered preparative HPLC (pump: Labomatic HD-5000 or HD-3000, head HDK 280, lowpressure gradient module ND-B1000; manual injection valve: Rheodyne 3725i038; detector: Knauer Azura UVD 2.15; collector: Labomatic Labocol Vario-4000; column: Chromatorex RP C-18 10 μm, 125×30 mm, flow: 70 mL/min) Acidic conditions: Eluent A: water+0.1 vol-% formic acid, Eluent B: acetonitrile+0.1 vol-% formic acid; Basic conditions: Eluent A: water+0.2 Vol-% aqueous ammonia (32%), Eluent B: acetonitrile; Experimental Section—General Procedures General Details All reactions were carried out under nitrogen (N2) atmosphere. ..

Injection:

Article Title: Dihydrooxadiazinones
Article Snippet: Nuclear magnetic resonance (NMR) spectra were recorded on a Bruker (300 or 400 MHz 1H, 75 or 101 MHz 13C) spectrometer. .. Preparative LC-MS Methods: Unless otherwise noted compounds were purified using mass-triggered preparative HPLC (Waters Autopurificationsystem; Column: Waters XBridge C18 5μ 100×30 mm; DAD scan: 210-400 nm, flow: 150 mL/min) or UV triggered preparative HPLC (pump: Labomatic HD-5000 or HD-3000, head HDK 280, lowpressure gradient module ND-B1000; manual injection valve: Rheodyne 3725i038; detector: Knauer Azura UVD 2.15; collector: Labomatic Labocol Vario-4000; column: Chromatorex RP C-18 10 μm, 125×30 mm, flow: 70 mL/min) Acidic conditions: Eluent A: water+0.1 vol-% formic acid, Eluent B: acetonitrile+0.1 vol-% formic acid; Basic conditions: Eluent A: water+0.2 Vol-% aqueous ammonia (32%), Eluent B: acetonitrile; Experimental Section—General Procedures General Details All reactions were carried out under nitrogen (N2) atmosphere. ..



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